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NanoMaterials Characterization

Nanotechnology is the science of manipulating materials at the atomic and molecular level to develop new or enhanced materials and products. MCLinc’s microscopy laboratory has the tools required for Nanomaterials characterization for research and development or prototype manufacturing.  Our state-of-the-art capabilities include and scanning electron microscopy (SEM) and transmission electron microscopy (TEM) with energy dispersive x-ray spectroscopy (EDS) and wavelength dispersive x-ray spectroscopy (WDS).

MCLinc has five electron microscopes including a JEOL 2000FX transmission electron microscope with 0.5 nanometer resolution and a maximum magnification of 1,000,000x, a Hitachi S-5000 scanning electron microscope with 0.6 nanometer resolution and a maximum magnification of 1,000,000x, a Hitachi S-4500 scanning electron microscope with 1.5 nanometer resolution and a maximum magnification of 500,000x, an Electroscope Corporation environmental scanning electron microscope (ESEM) with 4 nanometer resolution and a maximum magnification of 300,000x, and a JEOL JXA 840 scanning electron microscope with 4 nanometer resolution and a maximum magnification  of 300,000x. MCLinc’s ESEM system is a unique SEM instrument that allows the sample to be subjected to low-pressure gas conditions (water vapor and other gases) at pressures up to 25 torr.  This allows the observation of reactions between nanomaterials and water vapor or selected other gases. 

MCLinc has the experience and instrumentation required to  characterize bulk materials used in nanomaterials manufacturing.  MCLinc utilizes a collection of techniques including x-ray photoelectron spectroscopy (XPS), x-ray diffraction (XRD), x-ray fluorescence (XRF) and ICP-OES to provide elemental, chemical state, morphological and speciation analyses.  MCLinc’s x-ray photoelectron spectrometer, for example, provides surface analysis at 20 to 40 angstrom depth. 

Materials and Chemistry Laboratory, Inc.
East Tennessee Technology Park, Bldg. K-1006 • Oak Ridge, TN 37830-1702
Voice: (865) 576-4138 • FAX: (865) 576-8558
Contact:
Barry A. Stephenson
, President

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